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ChemistryIonic Equilibrium
In a qualitative analysis Bi³⁺ is detected by appearance of precipitate of BiO(OH)(s). Calculate pH when the following equilibrium exists at 298 K :
BiO(OH)(s) ⇌ BiO⁺(aq) + OH⁻(aq), K = 4 × 10⁻¹⁰
(Given: log 2 = 0·3010)
Options
1
4·699
2
8·714
3
9·301
4
5·286
Correct Answer
Option 3 : pH = 9·301
Step-by-Step Solution
1

Equilibrium expression:

BiO(OH)(s) ⇌ BiO⁺(aq) + OH⁻(aq)

K = [BiO⁺][OH⁻] = 4 × 10⁻¹⁰

(Pure solid BiO(OH) is not included in K expression)

2

Let solubility = s mol/L:

[BiO⁺] = s and [OH⁻] = s

s² = 4 × 10⁻¹⁰

s = √(4 × 10⁻¹⁰) = 2 × 10⁻⁵ mol/L

3

Calculate pOH:

[OH⁻] = 2 × 10⁻⁵

pOH = −log(2 × 10⁻⁵) = −log 2 − log 10⁻⁵ = −0·3010 + 5 = 4·699

4

Calculate pH:

pH + pOH = 14

pH = 14 − 4·699 = 9·301

s = 2×10⁻⁵ M → [OH⁻] = 2×10⁻⁵

pOH = 5 − log2 = 5 − 0·301 = 4·699

pH = 14 − 4·699 = 9·301

Theory: Ionic Equilibrium & pH Calculations
1. Solubility Product (Ksp)

For a sparingly soluble salt AxBy dissolving in water: AxBy(s) ⇌ xAʸ⁺(aq) + yBˣ⁻(aq). Ksp = [Aʸ⁺]ˣ[Bˣ⁻]ʸ. The solid phase is not included in Ksp (activity of pure solid = 1). In this problem, BiO(OH) is a sparingly soluble compound — the equilibrium involves its dissolution into BiO⁺ and OH⁻ ions. K = [BiO⁺][OH⁻] = Ksp = 4×10⁻¹⁰. Lower Ksp → less soluble → less ions in solution.

2. Relationship Between Solubility and Ksp

📌 AB type (1:1): Ksp = s² → s = √Ksp

📌 AB₂ or A₂B type (1:2 or 2:1): Ksp = 4s³ → s = (Ksp/4)^(1/3)

📌 A₂B₃ or A₃B₂ type (2:3 or 3:2): Ksp = 108s⁵ → s = (Ksp/108)^(1/5)

📌 This problem: BiO(OH) → BiO⁺ + OH⁻ (1:1 type) → Ksp = s²

📌 s = √(4×10⁻¹⁰) = 2×10⁻⁵ mol/L

3. pH, pOH and Their Relationship

pH = −log[H⁺] and pOH = −log[OH⁻]. At 25°C (298K): Kw = [H⁺][OH⁻] = 10⁻¹⁴. Taking −log: pH + pOH = 14. This relationship holds at 25°C only — at higher temperatures Kw increases so pH + pOH < 14. Neutral solution at 25°C: pH = 7 (neither acidic nor basic). Acidic: pH < 7. Basic: pH > 7. In this problem, [OH⁻] = 2×10⁻⁵ → basic solution → pH > 7 → pH = 9·301 ✓ (consistent with basic BiO(OH) dissolution).

4. Common Ion Effect on Solubility

Adding a common ion to a solution of sparingly soluble salt decreases its solubility (Le Chatelier's principle). Example: Adding NaOH (provides OH⁻) to BiO(OH) solution shifts equilibrium left → less BiO(OH) dissolves → lower solubility. Adding BiONO₃ (provides BiO⁺) also decreases solubility. The common ion effect is widely used in qualitative analysis to selectively precipitate ions. In this problem, if the solution already contained OH⁻ from another source, the solubility of BiO(OH) would be even lower.

5. Buffer Solutions — Henderson-Hasselbalch Equation

A buffer resists change in pH on addition of small amounts of acid or base. Consists of a weak acid + its conjugate base (or weak base + conjugate acid). Henderson-Hasselbalch: pH = pKa + log([A⁻]/[HA]). For basic buffer: pOH = pKb + log([Salt]/[Base]). Buffer capacity is maximum when [A⁻] = [HA], i.e., pH = pKa (or [Salt] = [Base], pOH = pKb). Biological buffers: blood pH 7·35–7·45 maintained by H₂CO₃/HCO₃⁻ buffer system. Phosphate buffer: H₂PO₄⁻/HPO₄²⁻.

6. Qualitative Analysis — Group Separations

Bi³⁺ belongs to Group II of qualitative analysis (precipitated as sulphides in the presence of H₂S at low pH). However, this question involves detection via BiO(OH) precipitation in alkaline conditions. Qualitative analysis uses differences in Ksp values to selectively precipitate ions. By controlling pH and the precipitating agent, different groups of cations are separated. Group I (HCl): Pb²⁺, Ag⁺, Hg₂²⁺ precipitate as chlorides. Group II (H₂S, acidic): Cu²⁺, Bi³⁺, Hg²⁺ as sulphides. Group III (NH₃): Fe³⁺, Al³⁺, Cr³⁺ as hydroxides.

7. Degree of Hydrolysis and Hydrolysis Constant

Salts of weak acid + strong base hydrolyse to give basic solution. Salts of strong acid + weak base hydrolyse to give acidic solution. Hydrolysis constant Kh = Kw/Ka (for salt of weak acid + strong base). Degree of hydrolysis h = √(Kw/Ka·C) for very dilute solutions or weak acids. pH of salt solution: for CH₃COONa: pH = 7 + ½(pKa + log C); for NH₄Cl: pH = 7 − ½(pKb + log C). These formulas are important for NEET numerical problems.

8. Ionic Product of Water and Effect of Temperature

Kw = [H⁺][OH⁻]. At 25°C: Kw = 10⁻¹⁴, pH of neutral water = 7. At 37°C (body temperature): Kw ≈ 2·4×10⁻¹⁴, neutral pH ≈ 6·8 (still neutral, but not 7). At 100°C: Kw ≈ 10⁻¹², neutral pH = 6. Dissolution of water is endothermic → increasing temperature increases Kw (more dissociation). This is a highly tested NEET concept: neutral solution always has [H⁺] = [OH⁻], but the neutral pH is 7 ONLY at 25°C.

Frequently Asked Questions
1. Why is BiO(OH)(s) not included in the K expression?
Pure solids and pure liquids have constant activity = 1 by convention, so they are not included in equilibrium constant expressions. BiO(OH) is a solid — its "concentration" doesn't change as long as some solid is present. Only species in solution (aq) or gas phase (g) appear in K expressions. Thus K = [BiO⁺][OH⁻] (just the aqueous ions).
2. Why is the answer 9·301 and not 4·699?
4·699 is the pOH, not the pH. The question asks for pH. pH = 14 − pOH = 14 − 4·699 = 9·301. This is a very common mistake — confusing pH and pOH. Always check: since BiO(OH) produces OH⁻ ions, the solution is basic → pH must be > 7. Option 4·699 is < 7 (acidic) → wrong. Option 9·301 > 7 (basic) → correct.
3. How is log(2×10⁻⁵) = −4·699 calculated?
pOH = −log[OH⁻] = −log(2×10⁻⁵). Using log rules: log(2×10⁻⁵) = log 2 + log 10⁻⁵ = 0·3010 + (−5) = −4·699. Therefore pOH = −(−4·699) = 4·699. The given hint "log 2 = 0·3010" is specifically for this step. Always use: −log(a × 10ⁿ) = −log a − n·log10 = −log a + |n|.
4. What is the common ion effect?
Adding an ion that is already present in the equilibrium shifts it to the left (Le Chatelier). For BiO(OH): adding NaOH (OH⁻ source) increases [OH⁻] → equilibrium shifts left → less BiO(OH) dissolves → solubility decreases. This principle is used in analytical chemistry to ensure complete precipitation (add excess of precipitating agent). It's also why milk of magnesia (Mg(OH)₂) is less soluble in alkaline conditions.
5. At what temperature is neutral pH NOT equal to 7?
Neutral pH = 7 only at 25°C (where Kw = 10⁻¹⁴). At any other temperature: Kw changes, so neutral pH = ½ × pKw. At 37°C: Kw ≈ 2·4×10⁻¹⁴, pKw ≈ 13·62, neutral pH ≈ 6·81. At 100°C: Kw ≈ 10⁻¹², pKw = 12, neutral pH = 6. In all cases, neutral means [H⁺] = [OH⁻] — the numerical value of neutral pH changes with temperature, but the concept (equal concentrations) does not.
6. What is the difference between Ksp and solubility?
Ksp (solubility product) is an equilibrium constant — a dimensionless number (in simplified form: units of concentration^n) that depends only on temperature. Solubility (s) is the maximum amount of solute that can dissolve in a given volume at a specific temperature (mol/L or g/L). Relationship: Ksp = f(s) depending on the stoichiometry. A compound with higher Ksp is generally more soluble, but cannot compare Ksp values of salts with different formulas (e.g., AgCl vs Ag₂CrO₄) directly without converting to molar solubility.
7. How does pH affect solubility of metal hydroxides?
For metal hydroxide M(OH)n: Ksp = [Mⁿ⁺][OH⁻]ⁿ. In acidic solution: [OH⁻] is low → equilibrium shifts right → more M(OH)n dissolves → higher solubility. In alkaline solution: [OH⁻] is high (common ion) → equilibrium shifts left → less dissolves → lower solubility. This is why metal hydroxides precipitate in basic solutions and dissolve in acidic solutions. This principle is the basis of group separations in qualitative analysis.
8. What happens to pH when a buffer is diluted?
Diluting a buffer does NOT significantly change its pH — this is the key property of buffers. Henderson-Hasselbalch: pH = pKa + log([A⁻]/[HA]). On dilution, both [A⁻] and [HA] decrease by the same factor, so their ratio stays constant → pH stays constant. However, buffer capacity (ability to resist pH change) decreases on dilution because there are fewer moles of buffer components to neutralise added acid/base. At infinite dilution, buffer capacity → 0.
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